Microwaves in Organic Synthesis || Microwave-Assisted Reactions on Graphite

✍ Scribed by Loupy, André

• Publisher: Wiley-VCH Verlag GmbH & Co. KGaA
• Year: 2002
• Tongue: German
• Weight: 486 KB
• Category: Article
• ISBN-13: 9783527601776
• DOI: 10.1002/3527601775.ch7

✦ Synopsis

a Reagents used in equimolar amounts (entries 4±6) or in excess of diene, 5/1 (entries 2, 3), 3/1 (entry 7), 2/1 (entry 1) b Yield of isolated product relative to the minor reagent. c Sequential MW irradiation (SMWI); applied incident power; time and number of irradiations; interval between two irradiations: 1 min (entries 1±3), 3 min (entries 4±7) d Reaction in sealed tube e Reaction performed in the presence of a catalyst: ZnCl 2 (entries 2, 7), AlCl 3 (entry 6) f Not given.