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Microwave promoted synthesis of cycl[3.2.2]azines in water via a new three-component reaction

✍ Scribed by Shyamalee Gogoi; Mandakini Dutta; Junali Gogoi; Romesh Chandra Boruah

Book ID: 104098741
Publisher: Elsevier Science
Year: 2011
Tongue: French
Weight: 549 KB
Volume: 52
Category: Article
ISSN: 0040-4039
DOI: 10.1016/j.tetlet.2010.12.036

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✦ Synopsis

A microwave-promoted and base-catalyzed synthesis of cycl[3.2.2]azines is accomplished in water via a three-component reaction (3-CR) of 2-picoline, a-bromoacetophenone and alkyne. The extension of the methodology to the synthesis of steroidal and carbocyclic cycl[3.2.2]azine is also reported.

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