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Microwave-Promoted Synthesis of Bicyclic Azocine-β-Lactams from Bis(allenes)

✍ Scribed by Alcaide, Benito; Almendros, Pedro; Aragoncillo, Cristina; Fernández, Israel; Gómez-Campillos, Gonzalo


Book ID
125530749
Publisher
American Chemical Society
Year
2014
Tongue
English
Weight
545 KB
Volume
79
Category
Article
ISSN
0022-3263

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Ring-closure of 1,3-azadienes to 13-1actam rings is efficiently and quickly carried out under solvent-free conditions in an open-vessel microwave system. The synthesis of N-tert-butyldimethylsilyl azetidinones is reported.