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Microwave assisted Wolff rearrangement: A facile method for the synthesis of Fmoc-β-amino acids

✍ Scribed by Basanagoud S. Patil; Ganga-Ramu Vasanthakumar; Vommina V. Suresh Babu

Book ID
111539767
Publisher
Springer Netherlands
Year
2002
Tongue
English
Weight
57 KB
Volume
9
Category
Article
ISSN
1573-3149

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A convenient method for the synthesis of
A convenient method for the synthesis of norstatine derivatives fromN-Fmoc orN-Boc amino acids
✍ Saïd Kourtal; Joëlle Paris 📂 Article 📅 1996 🏛 Springer Netherlands 🌐 English ⚖ 360 KB

A new and convenient method for synthesizing norstatine derivatives has been developed. The key step is the preparation of propargylic alcohols from N-Fmoc or N-Boc amino aldehydes, followed by transformation to carboxylic acids after protection of the alcohols. The N-Boc-protected derivatives are c