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Microwave-assisted synthesis of sodium sulfonates precursors of sulfonyl chlorides and fluorides

โœ Scribed by Shakiru O. Alapafuja; Spyros P. Nikas; Vidyanand G. Shukla; Ioannis Papanastasiou; Alexandros Makriyannis


Book ID
104097032
Publisher
Elsevier Science
Year
2009
Tongue
French
Weight
243 KB
Volume
50
Category
Article
ISSN
0040-4039

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Microwave-assisted synthesis of sodium s
โœ Shakiru O. Alapafuja; Spyros P. Nikas; Vidyanand G. Shukla; Ioannis Papanastasio ๐Ÿ“‚ Article ๐Ÿ“… 2009 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 243 KB

We describe the use of a microwave reaction for the conversion of various bromides to sodium sulfonates that have been further elaborated to sulfonyl chlorides. This new approach leads to much improved yields and shorter reaction times. Representative sulfonyl chlorides serve as precursors for the r