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MICROWAVE ASSISTED SYNTHESIS OF NOVEL 1,2,4-TRIAZINES IN “DRY MEDIA”

✍ Scribed by Kidwai, Mazaahir; Sapra, Pooja; Bhushan, Kumar Ranjan; Misra, Preeti


Book ID
120808389
Publisher
Taylor and Francis Group
Year
2001
Tongue
English
Weight
118 KB
Volume
31
Category
Article
ISSN
0039-7911

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Microwave-Assisted Synthesis of Novel 1,
✍ Mazaahir Kidwai; Rajesh Kumar; Anil Srivastava; H.P. Gupta 📂 Article 📅 1998 🏛 Elsevier Science 🌐 English ⚖ 196 KB

A series of triazines have been synthesized starting from 5-alkyl-1,3,4-thiadiazole-2-thioles (1a-d). On reaction with ethyl bromoacetate in the presence of anhydrous K 2 CO 3 under microwave irradiation (MWI), these yielded corresponding esters (2a-d) which on hydrazinolysis under MWI produced (5-a