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Microwave-assisted solvent-free synthesis of iminothiazolines

โœ Scribed by Souad Kasmi; Jack Hamelin; Hadj Benhaoua

Book ID
108387109
Publisher
Elsevier Science
Year
1998
Tongue
French
Weight
165 KB
Volume
39
Category
Article
ISSN
0040-4039

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ChemInform Abstract: Microwave-Assisted
ChemInform Abstract: Microwave-Assisted Solvent-Free Synthesis of Iminothiazolines.
โœ S. KASMI; J. HAMELIN; H. BENHAOUA ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› John Wiley and Sons โš– 31 KB ๐Ÿ‘ 2 views

Microwave-Assisted Solvent-Free Synthesis of Iminothiazolines. -Thioureas (I) and ฮฑ-chloro ketones (II) are readily condensed to imino 4-thiazolines under microwave irradiation in solvent-free conditions. Hydrochloride precursors are obtained in the absence of Al 2 O 3 . -(KASMI, S.;

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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract, please click on HTML or PDF.

Microwave-assisted solvent-free parallel
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โœ Roger Olsson; Henrik C Hansen; Carl-Magnus Andersson ๐Ÿ“‚ Article ๐Ÿ“… 2000 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 58 KB

Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the libr