Microwave assisted one-pot tandem three-component synthesis of 2,4,5-triary1-2-4-dihydro-3H-1,2,4-triazol-3-one derivatives
β Scribed by Mohammadi, Bagher; Adib, Mehdi
- Book ID
- 121658828
- Publisher
- Chinese Electronic Periodical Services
- Year
- 2014
- Tongue
- English
- Weight
- 376 KB
- Volume
- 25
- Category
- Article
- ISSN
- 1001-8417
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## Abstract A series of 3βalkyl(aryl)β4β(__p__βhydroxyβphenyl)β4,5βdihydroβ1__H__β1,2,4βtriazolβ5βones **2** were obtained from the reaction of alkyl (aryl) ester ethoxycarbonyl hydrazones **1** with __p__βhydroxy aniline. The reaction of **1** with 1,4βdiamino benzene (1:1) to afford 3βalkyl(aryl)
In the molecule of the title compound, C 9 H 9 N 3 O, the dihedral angle between the planar rings is 7.49 (3) . In the crystal structure, intermolecular N-HΓ Γ ΓO hydrogen bonds link the molecules into dimers, which may be effective in the stabilization of the crystal structure.