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Microwave-Assisted Conversion of Nitriles to Thioamides in Solvent-Free Condition

✍ Scribed by Matloubi Moghaddam, Firouz; Hojabri, Leila; Dohendou, Mohammad

Book ID
120909397
Publisher
Taylor and Francis Group
Year
2003
Tongue
English
Weight
167 KB
Volume
33
Category
Article
ISSN
0039-7911

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Microwave-assisted solvent-free parallel
Microwave-assisted solvent-free parallel synthesis of thioamides
✍ Roger Olsson; Henrik C Hansen; Carl-Magnus Andersson πŸ“‚ Article πŸ“… 2000 πŸ› Elsevier Science 🌐 French βš– 58 KB

Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the libr