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Micro Syntheses with Tracer Elements. III. The Synthesis of Thiourea Labeled with C 14 and of Thiourea Labeled with S 35

✍ Scribed by Bills, C. Wayne; Ronzio, Anthony R.

Book ID
126414395
Publisher
American Chemical Society
Year
1950
Tongue
English
Weight
295 KB
Volume
72
Category
Article
ISSN
0002-7863

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Micro-scale preparation of 4-thiouracil
Micro-scale preparation of 4-thiouracil labelled with 14C or 14C + 35S
✍ J. Seda; L. I. Votruba; R. Tykva πŸ“‚ Article πŸ“… 1974 πŸ› John Wiley and Sons 🌐 French βš– 308 KB

## Abstract A selective and quantitative method was developed for a microscale preparation of 4‐thiouracil‐2‐^14^C by the direct thiation of uracil‐2‐^14^C. From pyridine, dioxane, and tetralin as the thiation solvents, the best yield was obtained in dioxane (96.6% of 4‐thiouracil‐2‐^14^C). The sim