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Methyl 4,6-O-benzylidene-2-deoxy-2-C-(1,2:3,4-di-O-isopropylidene-l-glycero-d-galacto-hexopyranos-6-yl)-α-d-arabino-hexopyranosid-3-ulose monohydrate

✍ Scribed by Ciunik, Z. ;Luger, P. ;Yu, K. L.

Book ID
114508984
Publisher
International Union of Crystallography
Year
1992
Tongue
English
Weight
460 KB
Volume
48
Category
Article
ISSN
0108-2701

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X-ray and conformational investigation o
X-ray and conformational investigation of 6-deoxy-6-C-(1,5-di-O-acetyl-2,3-O-isopropylidene-β-d-allo-pentofuranos-5-yl)-1,2:3,4-di-O-isopropylidene- α-d-galactopyranose and 6-C-(benzyl 5-deoxy-2,3-O-isopropylidene-β-d-ribofuranosid-5-yl)-1,2:3,4-di-O-isopropylidene- d-glycero-α-d-galacto-hexopyranose
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The structures of the title compounds (2b and 3) have been investigated in the solid state by X-ray methods. The crystals of 2b are monoclinic, space group P2,, and of 3 orthorhombit, space grtup P2,2,2,. The cell dimensions are: for 2b, a = 9.910(2), b = 11;745W, c = 11.810(3) A, /3 = 97.32(l)"; a

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6-C-(2-Furyl)-1,2:3,4-di-O-isopropylidene-~-D-g~yce~o-D-ga~~c~o-hexopyranose (1) has been investigated by X-ray diffraction methods. The crystals obtained from ethyl acetate-light petroleum were monoclinic, space group P2, (2 = 2)) with cell dimensions a = 13.796(2), b = 7.887(l), c = 8.035(l) A, an