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Methyl 3,6-an­hydro-4-azido-5,7-O-(S)-benzyl­idene-2,4-di­deoxy-d-talo-heptonate

✍ Scribed by Newton, Christopher R. ;Horne, Graeme ;Fleet, George W. J. ;Nash, Robert J. ;Cooper, Richard I.

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
261 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 15 H 17 N 3 O 5 , was formed by carrying out a Wittig reaction, under basic conditions, on 2-azido-3,5±Obenzylidene-2-deoxy-d-lyxose.

📜 SIMILAR VOLUMES

3-Azido-3-deoxy-2,2′:5,6-di-O-iso­propyl
3-Azido-3-deoxy-2,2′:5,6-di-O-iso­propyl­idene-2-C-hydro­xmethyl-d-gulono-1,4-lactone
✍ Harding, Christopher C. ;Shallard-Brown, Howard ;Watkin, David J. ;Soengas, Raqu 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 897 KB

Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.108 Data-to-parameter ratio = 9.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

5,6,7,9-Tetra-O-acetyl-4,8-an­hydro-1,2,
5,6,7,9-Tetra-O-acetyl-4,8-an­hydro-1,2,3-tri­deoxy-d-glycero-d-gulo-non-1-enitol
✍ Rhoad, Jonathon S. ;Lowary, Todd L. ;Ferguson, Michael J. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 196 KB

Single-crystal X-ray study T = 193 K Mean '(C±C) = 0.005 A Ê R factor = 0.053 wR factor = 0.100 Data-to-parameter ratio = 9.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.