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Methyl 3-[(E)-2-(4-bromo­benzoyl­methyl­idene)imidazolidin-1-yl]acrylate

✍ Scribed by Yu, Chu-Yi ;Gao, Hong-Yun ;Qiao, Yan

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
218 KB
Volume
62
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.014 A Ê R factor = 0.056 wR factor = 0.135 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C 9 H 12 N 2 O 3 , was synthesized by the reaction in ethanol of ethane-1,2-diamine and 3-[bis(methylthio)methylene]-6-methyl-3,4,5,6-tetrahydro-2H-pyran-2,4dione. Two intramolecular N-HÁ Á ÁO hydrogen bonds induce a high degree of planarity.

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diazenyl]phenol O ¨zdemir Gonca, a Is ¸ık S ¸amil, a C ¸ig ˘dem Albayrak b and Ag ˘ar Erbil b \*