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Methyl 2,6-anhydro-3-azido-4-O-benzoyl-3-deoxy-α-d-idopyranoside, a new 2,5-dioxabicyclo[2.2.2]octane derivative

✍ Scribed by Castellano, E. E. ;Oliveira, M. A. ;Baptistella, L. H. B. ;Marsaioli, A. J. ;Castillon, S. ;Lukacs, G.

Book ID
114503733
Publisher
International Union of Crystallography
Year
1986
Tongue
English
Weight
319 KB
Volume
42
Category
Article
ISSN
0108-2701

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The title compound (21) was synthesized from cellobiose as a synthon of a heparin-related oligosaccharide. The per-0-benzyl and per-0-benzoyl derivatives of 1 ,6-anhydro-4-0-(6-deoxy-B-D-~~~lo-hex-5-enopyranosyl)-~-~-glucopyranose were treated with a nonsolvated borane to give a 1 :2 mixture of the