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Metacyclophanes and related compounds. 18. Preparation of anti-5,14-di-tert-butyl-8,17-dimethyl[2.3]metacyclophan-1-ene and anti-5,15-di-tert-butyl-8,18-dimethyl[2.4]metacyclophan-1-enes with dichlorocarbene

✍ Scribed by Yamato, Takehiko; Kobayashi, Kazumasa; Arimura, Takashi; Tashiro, Masashi; Yoshihira, Kunitoshi; Kawazoe, Kayoko; Sato, Sadao; Tamura, Chihiro

Book ID
127237465
Publisher
American Chemical Society
Year
1986
Tongue
English
Weight
576 KB
Volume
51
Category
Article
ISSN
0022-3263

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in solvent or counterion R factor = 0.047 wR factor = 0.159 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.