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Metabolite structure elucidation using NMR micro-/nano-detection

โœ Scribed by John P. Shockcor; Robert M. Wurm; Ivin S. Silver; Ronald C. Crouch; Gary E. Martin


Publisher
Elsevier Science
Year
1994
Tongue
French
Weight
328 KB
Volume
35
Category
Article
ISSN
0040-4039

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โœฆ Synopsis


Abrtnzct: lbe struchrre of the epoxidc of l-ethyl-pbemxdih 10.1O-dioxMe+ a potcmtial monomim oxidase-A inhibiita, was elucidated usinr a cxmbinatim of 500 MHz bmo-ad hcdemnuclear NMR tfxMo~~. 'Ibe pmtom


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## Abstract A general and unambiguous approach has been developed for structural elucidation of modified purine nucleosides using NMR spectroscopy. Systematic assignment of proton and carbon signals of modified nucleosides was firmly established by COSY and the anomerism of the glycosidic linkage o