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Mass spectrometry of macroheterocycles. 1. Mass spectra of isomeric bicyclic crown ethers

✍ Scribed by A. I. Gren'; A. V. Mazepa; A. V. Lobach; N. G. Luk'yanenko; O. S. Timofeev


Publisher
Springer US
Year
1991
Tongue
English
Weight
340 KB
Volume
27
Category
Article
ISSN
0009-3122

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✦ Synopsis


extract was dried over CaCI 2 and evaporated in vacuo. The residue was purified by column chromatography [silica gel, benzene--ethyl acetate (5:1)] and recrystallized from benzene--heptane to give 1.98 g (48%) of III.


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