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Mass Spectrometer Appearance Potentials for Positive Ion Fragments from BF3, B(CH3)3, B(C2H5)3, B(OCH3)3, and HB(OCH3)2

✍ Scribed by Law, Robert W.; Margrave, John L.

Book ID
120424207
Publisher
American Institute of Physics
Year
1956
Tongue
English
Weight
452 KB
Volume
25
Category
Article
ISSN
0021-9606

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Trimethylamine-bis(trifluoromethyl) boranes R(CF 3 ) 2 B Β΄NMe 3 (R = cis/trans-CF 3 CF=CF (1/2), HCΒΊC (3), H 2 C=CH (4), C 2 H 5 (5), C 6 H 5 CH 2 (6), C 6 F 5 (7), C 6 H 5 (8)) react with NEt 3 Β΄3 HF depending on the nature of R at 155Β±200 Β°C under replacement of the trimethylamine ligand to form