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Mass-spectral Study of 9-[α(β,γ)-Picolylidene]-1(4)-azafluorenes

✍ Scribed by P. I. Zakharov; N. M. Kolyadina; N. S. Prostakov; Mazhed Gassan; N. I. Golovtsov

Book ID
110363752
Publisher
Springer US
Year
2000
Tongue
English
Weight
120 KB
Volume
36
Category
Article
ISSN
0009-3122

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~)-l-Methyl-l,2,3~4-tetrahydroisoquinoline (I). A mixture of 0.04 mole of compound IV, 0.09 mole of AICI s, and 150 ml of decaline distilled from over sodium is heated for three hours at 145-150~ After the end of the heating, the reaction mixture is decomposed with ice and conc. HCI, the decaline l