Mass spectra of negative ions of nitrones and isomeric O-ethers of oximes
β Scribed by R. G. Kostyanovskii; A. P. Pleshkova; V. N. Voznesenskii; V. I. Khovstenko; A. Sh. Sultanov; V. K. Mavrodiev; A. I. Mishchenko; A. V. Prosyanik
- Book ID
- 112442234
- Publisher
- Springer
- Year
- 1979
- Tongue
- English
- Weight
- 234 KB
- Volume
- 28
- Category
- Article
- ISSN
- 1573-9171
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## Abstract Comparative studies of the ionisation potentials and the mass spectra of some isomeric nitrones, oxaziranes, __O__βether oximes and acid amides gave no evidence for hermallyβinduced isomerisation in the mass spectrometer. Characteristic differences in the electronβimpactβinduced fragmen
extract was dried over CaCI 2 and evaporated in vacuo. The residue was purified by column chromatography [silica gel, benzene--ethyl acetate (5:1)] and recrystallized from benzene--heptane to give 1.98 g (48%) of III.