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Mass spectra of n-butylboronate ester derivatives of the major metabolite of prostaglandin F

โœ Scribed by Aldo Ferretti; Vincent P. Flanagan; John M. Roman

Publisher
John Wiley and Sons
Year
1994
Tongue
English
Weight
462 KB
Volume
29
Category
Article
ISSN
1076-5174

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โœฆ Synopsis

Abstract

The EI mass spectra of six nโ€butylboronate ester derivatives of the major metabolite of prostaglandins F~1ฮฑ~ and F~2ฮฑ~ (PGFโ€M) are presented and discussed. Proposed ion assignments and fragmentation pathways are based on substituent shifts, on data from a deuteriumโ€labeled methoxime derivative and on the analysis of collisionโ€induced dissociation spectra of selected ions. Fragment ions suitable for identification and quantification of PGFโ€M in a biological matrix and diagnostically valuable ions for structure recognition are proposed.

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