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Marfey’s reagent for chiral amino acid analysis: A review

✍ Scribed by R. Bhushan; H. Brückner

Publisher
Springer
Year
2004
Tongue
English
Weight
246 KB
Volume
27
Category
Article
ISSN
0939-4451

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Use of Marfey's reagent to quantitate ra
Use of Marfey's reagent to quantitate racemization upon anchoring of amino acids to solid supports for peptide synthesis
✍ J. Gordon Adamson; Thang Hoang; Anna Crivici; Gilles A. Lajoie 📂 Article 📅 1992 🏛 Elsevier Science 🌐 English ⚖ 517 KB

A chromatographic assay has been developed to quantitate racemization occurring during attachment of protected amino acids to peptide synthesis resins. Acidolytic cleavage of deprotected amino acids from supports and subsequent derivatization with 1-fluoro-2,4-dinitrophenyl-5-L-alanine amide (Marfey