Location of the O-acetyl group in welan by the reductive-cleavage method
β Scribed by John D. Stankowski; Samuel G. Zeller
- Book ID
- 107727172
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 326 KB
- Volume
- 224
- Category
- Article
- ISSN
- 0008-6215
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π SIMILAR VOLUMES
Described herein are methods for determining the degree of substitution (ds) and the positions of substitution of O-acetyl groups in commercial samples of partially O-acetylated cellulose. Sequential neutral methylation of the polymers, base-catalyzed ethylation, and reductive cleavage gives eight p
Agarose was structurally characterised by permethylation and subsequent reductive cleavage. Treatment of the fully methylated polysaccharide with triethylsilane and a mixture of trimethylsilyl methanesulfonate and boron trifluoride etherate followed by a newly developed, acid-catalysed, in situ acet
A method is described for the analysis of positions of substitution of O-carboxylated groups in commercial samples of O-carboxymethylcellulose. Sequential permethylation of the polymer and reductive cleavage gives eight products, which are analyzed as their O-acetyl derivatives by gas-liquid chromat