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Analysis of positions of substitution of O-carboxymethyl groups in partially O-carboxymethylated cellulose by the reductive-cleavage method

✍ Scribed by Samuel G. Zeller; George W. Greisgraber; Gary R. Gray

Publisher: Elsevier Science
Year: 1991
Tongue: English
Weight: 350 KB
Volume: 211
Category: Article
ISSN: 0008-6215
DOI: 10.1016/0008-6215(91)84144-4

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✦ Synopsis

A method is described for the analysis of positions of substitution of O-carboxylated groups in commercial samples of O-carboxymethylcellulose. Sequential permethylation of the polymer and reductive cleavage gives eight products, which are analyzed as their O-acetyl derivatives by gas-liquid chromatography.

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