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Living and Controlled Anionic Polymerization of Methacrylates and Acrylates in the Presence of Tetraalkylammonium Halide–Alkylaluminum Complexes in Toluene

✍ Scribed by Helmut Schlaad; Bardo Schmitt; Axel H. E. Müller

Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
93 KB
Volume
37
Category
Article
ISSN
0044-8249

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New initiator system for the anionic polymerization of (meth)acrylates in toluene. IV. Random copolymerization of (meth)acrylates in toluene initiated by s-BuLi ligated by lithium silanolates
✍ Catherine Zune; Thomas Zundel; Philippe Dubois; Philippe Teyssié; Robert Jérôme 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 155 KB 👁 2 views

Copolymerization of binary mixtures of alkyl (meth)acrylates has been initiated in toluene by a mixed complex of lithium silanolate O(s-BuMe 2 SiOLi)O and s-BuLi (molar ratio Ͼ 21) formed in situ by reaction of s-BuLi with hexamethylcyclotrisiloxane (D 3 ). Fully acrylate and methacrylate copolymers