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Liquid chromatographic separation of the enantiomers of β-amino acids on a ligand exchange chiral stationary phase

✍ Scribed by Myung Ho Hyun; Sang Cheol Han; Sung Hee Whangbo

Publisher
John Wiley and Sons
Year
2003
Tongue
English
Weight
78 KB
Volume
17
Category
Article
ISSN
0269-3879

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✦ Synopsis

A liquid chromatographic ligand exchange chiral stationary phase (CSP) derived from (S)-leucinol was applied in the separation of the enantiomers of 12 beta-amino acids. The resolution was quite successful especially for the enantiomers of beta-amino acids containing aromatic functional group in the side chain. The chromatographic resolution behaviors were dependent on the organic modifier and Cu(II) concentration in aqueous mobile phase and the column temperature.

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