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Liquid chromatographic resolution of racemic ketones as their oxime 3,5-dinitrophenyl carbamates on a chiral stationary phase

โœ Scribed by Myung Ho Hyun; Young-Whan Park; In-Kyu Baik


Book ID
108381722
Publisher
Elsevier Science
Year
1988
Tongue
French
Weight
255 KB
Volume
29
Category
Article
ISSN
0040-4039

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A chiral stationary phase (CSP 2) was prepared by connecting N-(3,5-dinitrobenzoyl)-(R)-phenylglycinol to silica gel through carbamate linkage. The CSP was applied in resolving racemic N-acyl-1-arylaminoalkanes and the chromatographic resolution results were compared with those on the previously rep