Liquid chromatographic enantiomer resolution of N-hydrazide derivatives of 2-aryloxypropionic acids on a crown ether derived chiral stationary phase
β Scribed by Jing Yu Jin; Wonjae Lee
- Publisher
- John Wiley and Sons
- Year
- 2006
- Tongue
- English
- Weight
- 110 KB
- Volume
- 19
- Category
- Article
- ISSN
- 0899-0042
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## Liquid chromatographic direct resolution of b-amino acids on a chiral crown ether stationary phase A chiral stationary phase (CSP) prepared by bonding (+)-(18-crown-6)-2,3,11,12tetracarboxylic acid to silica gel was used for the direct resolution of b-amino acids. To determine the optimum mobil
## Abstract The liquid chromatographic enantiomer separation of __N__βfluorenylmethoxycarbonyl (FMOC) protected Ξ±βamino acids and their ethyl ester derivatives was performed on polysaccharideβderived chiral stationary phases, Chiralcel OD, Chiralpak AD, and Chiralpak AS. In general, Chiralcel OD an