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Lipoxin A4: Problems with its determination using reversed phase chromatography–tandem mass spectrometry and confirmation with chiral chromatography

✍ Scribed by Ferreirós, Nerea; Homann, Julia; Labocha, Sandra; Grossmann, Nina; Hahn, Julia S.; Brüne, Bernhard; Geisslinger, Gerd

Book ID: 122152950
Publisher: Elsevier Science
Year: 2014
Tongue: English
Weight: 415 KB
Volume: 127
Category: Article
ISSN: 0039-9140
DOI: 10.1016/j.talanta.2014.03.051

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## Abstract A sensitive, specific and rapid liquid chromatography–mass spectrometry (LC‐MS/MS) method has been developed and validated for enantioselective determination of darusentan enantiomers, orally active potent endothelin‐A receptor antagonist, in rat plasma. The plasma samples were pretreat