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Lipase catalyzed resolution of chiral acids or alcohols using mixed carboxylic-carbonic anhydrides

✍ Scribed by Eryka Guibé-Jampel; Zbigniew Chalecki; Mohamed Bassir; Mirjana Gelo-Pujic

Book ID
107857794
Publisher
Elsevier Science
Year
1996
Tongue
French
Weight
344 KB
Volume
52
Category
Article
ISSN
0040-4020

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Lipase-catalyzed resolution of primary a
Lipase-catalyzed resolution of primary alcohol containing quaternary chiral carbon
✍ Chan Seong Cheong; Dai Sig Im; Jiyoung Kim; In O Kim 📂 Article 📅 1996 🏛 Springer Netherlands 🌐 English ⚖ 279 KB

2-Cyano-2-phenyl-I-hexanol containing chiral quatemary carbon was resolved using a lipase. Among various reaction conditions, transesterification reaction (solvent; n-hexane, lipase; Candida cylindracea) gave high selectivity(20/80). Additionally, the selectivity could be improved( 13187) when pyrid