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LiOAc-Catalyzed Chemoselective Deprotection of Aryl Silyl Ethers under Mild Conditions

✍ Scribed by Wang, Bing; Sun, Hui-Xia; Sun, Zhi-Hua

Book ID
120243030
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
139 KB
Volume
74
Category
Article
ISSN
0022-3263

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A series of acetonides (both terminal and internal isopropylidene acetals) have been deprotected under catalytic, neutral conditions to give their corresponding 1,2-diols. The reactions utilize indium(III) triflate in the presence of water and an organic solvent with mild microwave heating. Terminal