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Large scale synthesis of bilirubin-XIIIα from IXα

✍ Scribed by M. Reisinger; F. R. Trull; D. A. Lightner

Book ID
112127975
Publisher
Journal of Heterocyclic Chemistry
Year
1985
Tongue
English
Weight
166 KB
Volume
22
Category
Article
ISSN
0022-152X

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The synthesis of [10-13C]bilirubin IXα
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## Abstract The total synthesis of [10‐^13^C]bilirubin IXα, the principal waste product of haem degradation, is described. Site specific labelling was accomplished by the Vilsmeier formylation of one of the dipyrrolic fragments using [1‐^13^C]dimethylformamide. The penultimate dehydrohalogenation r

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## Abstract The three structural isomers bilirubin IXα (**1a**), IIIα (**2a**), and XIIIα (**3a**) have been separated on a preparative scale by high‐performance low‐pressure liquid chromatography. They were converted into their dimethyl esters **1b, 2b**, and **3b** and characterized by UV, IR, MS