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Kristalline und molekulare Struktur von N-Isopropyl-7endo-phenyl-5,9-methano-6,7,8,9-tetrahydro-5 H-benzo-cyclohepten-6exo-yl-amin

✍ Scribed by Hans Peter Weber; Trevor James Petcher

Publisher: John Wiley and Sons
Year: 1978
Tongue: German
Weight: 192 KB
Volume: 61
Category: Article
ISSN: 0018-019X
DOI: 10.1002/hlca.19780610212

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✦ Synopsis

Crystal and Molecular Structure of N‐Isopropyl‐7__endo__‐phenyl‐5,9‐methano‐6,7,8,9‐tetrahydrobenzocyclo‐hepten‐6__exo__‐yl‐amin

The structure of the title compound was determined by X‐ray analysis of its hydrochloride. Space group Iba2, a=32.58, b=15.55, c=7.30 Å. The structure was refined by LS‐methods with 718 significant data to R=0.053.

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✍ Föhlisch, Baldur ;Schupp, Eberhard ;Dukek, Ursula ;Graeßle, Irmela 📂 Article 📅 1973 🏛 Wiley (John Wiley & Sons) ⚖ 559 KB

## Abstract Die 7‐Oxo‐7__H__‐benzocyclohepten‐6,8‐dicarbonsäureester **1** reagieren mit Malodinitril, Cyanessigäure‐methylester und Äthan‐1,1,2,2‐tetracarbonitril in Gegenwart katalytischer Mengen Diäthylamin zu den substituierten 5,9‐Methano‐ oder 5,9‐Äthano‐8,9‐dihydro‐5__H__‐benzocycloheptenen