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Kinetics of the reactions of p-nitrophenylbis(chloromethyl)phosphinate with primary and secondary amines

✍ Scribed by V. E. Bel'skii; L. S. Novikova; L. A. Kudryavtseva; B. E. Ivanov

Book ID
112487447
Publisher
Springer
Year
1977
Tongue
English
Weight
276 KB
Volume
26
Category
Article
ISSN
1573-9171

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The nature of the products from the reaction of TrtPH 2 (1) with an equimolar amount of phosgene strongly depends on the solvent. The initial intermediate 2 was isolated from toluene, but lost CO in dichloromethane, and HCl in diethyl ether, yielding TrtP(H)Cl (3), and (TrtPCO) 2 (4 b), respectively