Kinetics of microwave-assisted polymerization of ϵ-caprolactone
✍ Scribed by G. Sivalingam; Nitin Agarwal; Giridhar Madras
- Publisher
- John Wiley and Sons
- Year
- 2003
- Tongue
- English
- Weight
- 132 KB
- Volume
- 91
- Category
- Article
- ISSN
- 0021-8995
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📜 SIMILAR VOLUMES
Microwave irradiation was applied to synthesize poly(-caprolactam-co-caprolactone) directly from the anionic catalyzed ring opening of two cyclic monomers, -caprolactam and -caprolactone using a variable frequency microwave furnace, programmed to a set temperature and controlled by a pulsed power on
High-molecular-weight polymers of ⑀-caprolactone (CL) and maleic anhydride (MA) with anhydride group content of about 1% wt have been synthesized and studied. The polymerization reaction was carried out in bulk under nitrogen atmosphere. Stannous octoate (Sn(oct) 2 ), and 2,2'-azobisisobutyronitrile