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J-Compensated Proton-Detected Heteronuclear Shift-Correlation Experiments

✍ Scribed by A.M. Torres; T.T. Nakashima; R.E.D. Mcclung


Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
566 KB
Volume
102
Category
Article
ISSN
1064-1858

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Experiments to Detect Long-Range Heteron
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The utility of the J-HSMQC experiment to detect long-range CH correlations was investigated. Two new long-range J-compensated pulse sequences, LR-J-HSMQC(80,27) and LR-J-HSMQC(27,80), were developed using the (3beta(x))beta(y) composite 90 degrees pulse sequence. These two experiments were shown to