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Isothiocyanates. A new class of uncouplers

✍ Scribed by M. Miko; B. Chance

Book ID: 115716473
Publisher: Elsevier Science
Year: 1975
Tongue: English
Weight: 516 KB
Volume: 396
Category: Article
ISSN: 0005-2728
DOI: 10.1016/0005-2728(75)90031-6

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Method 1): (3a) is heated in 80 % H z S 0 4 at 150 OC for 112 h. On cooling and dilution, ( l a ) is precipitated; it was recrystallized from H20. Method 2): 1 g of (4a) and 2 ml of 52 % hydrazine are dissolved in alcohol; (la) is precipitated after ca. 12 h. (4a) is dissolved in hot alcohol and t