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Isolation of saikogenin E, a new triterpene from Bupleurum Falcatum L.

✍ Scribed by Tokuo Kubota; Hiroshi Hinoh

Publisher: Elsevier Science
Year: 1966
Tongue: French
Weight: 141 KB
Volume: 7
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)72932-7

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✦ Synopsis

In o recent communication (I), we have described that acid hydrolysis of the crude saponin obtained from the root of Bupleurum falcotum L. afforded four new

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We report here a successful example of organic structure determination whichrequires several steps of chemical procedure and has readily been performed using 13C NMR spectroscopy without chemical degradations. Triterpenoid glycosides, saikosaponin-a (3, -b,--b,, -c, -d (2, and -f were already isolat

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## Abstract Centrifugal partition chromatography (CPC) coupled with evaporative light scattering detection (ELSD) was applied to separate saikosaponins‐a and ‐c preparatively from __Bupleurum falcatum__ roots. The two‐phase solvent system composed of ethyl acetate/__n__‐butanol/methanol/water (15:1