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Isolation and Structural Characterization of 1-Zirconacyclopent-3-yne, Five-Membered Cyclic Alkynes

✍ Scribed by Suzuki, N.

Book ID
127278981
Publisher
American Association for the Advancement of Science
Year
2002
Tongue
English
Weight
161 KB
Volume
295
Category
Article
ISSN
0036-8075

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πŸ“œ SIMILAR VOLUMES

Transformation of a 1-Zirconacyclopent-3
Transformation of a 1-Zirconacyclopent-3-yne, a Five-Membered Cycloalkyne, into a 1-Zirconacyclopent-3-ene and Formal β€œ1-Zirconacyclopenta-2,3-dienes”
✍ Noriyuki Suzuki; Daisuke Hashizume; Hiroyuki Koshino; Teiji Chihara πŸ“‚ Article πŸ“… 2008 πŸ› John Wiley and Sons 🌐 English βš– 345 KB πŸ‘ 1 views

Preparation of 8 a: Complex 3 (75.3 mg, 0.105 mmol) and KC 8 (46 mg; K atoms: 0.25 mmol) were suspended in THF (1.5 mL) at room temperature, and the resulting mixture was stirred for 1 h. The deep blue mixture was then cooled to Γ€78 8C, and iodomethane (68 mg, 0.48 mmol) was added dropwise. The mixt

Transformation of a 1-Zirconacyclopent-3
Transformation of a 1-Zirconacyclopent-3-yne, a Five-Membered Cycloalkyne, into a 1-Zirconacyclopent-3-ene and Formal β€œ1-Zirconacyclopenta-2,3-dienes”
✍ Noriyuki Suzuki; Daisuke Hashizume; Hiroyuki Koshino; Teiji Chihara πŸ“‚ Article πŸ“… 2008 πŸ› John Wiley and Sons 🌐 English βš– 345 KB πŸ‘ 1 views

Preparation of 8 a: Complex 3 (75.3 mg, 0.105 mmol) and KC 8 (46 mg; K atoms: 0.25 mmol) were suspended in THF (1.5 mL) at room temperature, and the resulting mixture was stirred for 1 h. The deep blue mixture was then cooled to Γ€78 8C, and iodomethane (68 mg, 0.48 mmol) was added dropwise. The mixt