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Isolation and Stereochemical Studies of a Cyclic Alkoxysulfonium Salt, an Important Intermediate in the Nucleophilic Reaction of Chlorooxasulfuranes

✍ Scribed by Zhang, Jian; Saito, Shinichi; Koizumi, Toru

Book ID: 126903889
Publisher: American Chemical Society
Year: 1998
Tongue: English
Weight: 57 KB
Volume: 63
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo980314t

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## Abstract We report time‐resolved resonance Raman spectra for the azirine intermediate produced in the 2‐fluorenylnitrene ring‐expansion reaction to form a dehydroazepine product. The Raman bands obtained with a 252.7 nm probe wavelength and 500 ns delay time exhibit reasonable agreement with pre