✦ LIBER ✦

Investigation of graphite-probe atomisation for carbon-furnace atomic emission spectrometry

✍ Scribed by J. Marshall; S.K. Giri; D. Littlejohn; J.M. Ottaway

Publisher: Elsevier Science
Year: 1983
Tongue: English
Weight: 886 KB
Volume: 147
Category: Article
ISSN: 0003-2670
DOI: 10.1016/0003-2670(83)80082-8

No coin nor oath required. For personal study only.

✦ Synopsis

A new method of sample introduction for carbon furnace atomic emission spectrometry is described. The sample is deposited on a graphite probe which is inserted into the furnace along its length, after the tube has attained its maximum temperature. The heating rate experienced by the sample in an HGA-72 furnace is considerably increased by use of probe atomisation. Improved detection limits for a number of elements are reported, and the interference of magnesium chloride on the emission signals for lead and cadmium is substantially reduced.

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