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Investigation of Carbohydrate Conformation in Solution and in Powders by Double-Quantum NMR

✍ Scribed by Ravindranathan, Sapna; Feng, Xiaolong; Karlsson, Torgny; Widmalm, Göran; Levitt, Malcolm H.

Book ID
127022613
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
399 KB
Volume
122
Category
Article
ISSN
0002-7863

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✍ S. Ravindranathan; T. Karlsson; K. Lycknert; G. Widmalm; M.H. Levitt 📂 Article 📅 2001 🏛 Elsevier Science 🌐 English ⚖ 116 KB

Double-quantum heteronuclear local field NMR is performed on a sample of a 13C2-labeled disaccharide, in which the two 13C spins are located on opposite sides of the glycosidic linkage. The evolution of the double-quantum coherences is found to be consistent with the solid-state conformation of the