We report, for the first time, our experimental investigation of inverse phase suspension polymerization of acrylamide in a batch oscillatory baffled reactor. In such a reactor, the oscillatory motion is achieved by moving a set of orifice baffles up and down the column at the top of the reactor. Th
Inverse suspension polymerization of acrylamide
โ Scribed by M.V. Dimonie; C.M. Boghina; N.N. Marinescu; M.M. Marinescu; C.I. Cincu; C.G. Oprescu
- Publisher
- Elsevier Science
- Year
- 1982
- Tongue
- English
- Weight
- 868 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0014-3057
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โฆ Synopsis
The polymerization of acrylamide in inverse suspension is described and compared with polymerization in solution. The influences of various factors upon the molecular weight of the polymer were studied, viz. the concentration of initiator, the procedure of aqueous phase addition, the nature and concentration of emulsifier, the salt concentration, the time between mixing of phases and start of polymerization etc. Conductometry, NMR and electron microscopy were employed in order to establish the reaction stages and the characteristics of the polymers. The results indicate the importance of each factor and lead to an understanding of the polymerization.
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