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Introduction of the 3-Keto-▵ 4 -conjugated System in the Desoxycholic Acid Series

✍ Scribed by Riegel, Byron; McIntosh, A. Vern

Book ID
127000144
Publisher
American Chemical Society
Year
1944
Tongue
English
Weight
609 KB
Volume
66
Category
Article
ISSN
0002-7863

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3-(4-Oxocyclo­hexyl)propionic acid monoh
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✍ Witko, Stephanie M. ;Davison, Mark ;Thompson, Hugh W. ;Lalancette, Roger A. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 111 KB

In the title crystal structure, C~9~H~14~O~3~·H~2~O, the water molecule accepts a hydrogen bond from the carboxyl group [O...O = 2.6004 (13) Å and O—H...O = 163°], while donating hydrogen bonds to the ketone [O...O = 2.8193 (14) Å and O—H...O = 178 (2)°] and the acid carbonyl groups [O...O = 2.8010