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Intramolecular electron transfer. 3. Bis(4-pyridyl)methane as bridging group

✍ Scribed by Rieder, K.; Taube, H.

Book ID: 127353161
Publisher: American Chemical Society
Year: 1977
Tongue: English
Weight: 504 KB
Volume: 99
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00466a022

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Compound ( 1 ) (0.68g, 4mmol) is dissolved under N2 in anhydrous tetrahydrofuran (50 ml). To this solution, cooled to -113"C, is added dropwise a solution of tert-butyllithium in n-pentane (3ml,5.1 mmol; ca. 1.7 M solution). After 15min the olefin or carbonyl compound (8mmol) is addedC6]. The soluti