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Intestinal absorption and metabolism of 9-CIS-β-carotenein vivo: Biosynthesis of 9-CIS-retinoic acid

✍ Scribed by Hébuterne, X.; Wang, X-D; Johnson, E.J.; Krinsky, N.I.; Russell, R.M.

Book ID: 121989414
Publisher: Elsevier Science
Year: 1995
Tongue: English
Weight: 149 KB
Volume: 108
Category: Article
ISSN: 0016-5085
DOI: 10.1016/0016-5085(95)27227-5

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## Abstract 1‐[^13^CD~3~]‐9‐__cis__‐Retinoic acid was prepared in 8 steps from 2,6‐dimethylcyclohexanone. Alkylation of 2,6‐dimethylcyclohexanone under LiHMDS/MnBr~2~/^13^CD~3~I gave the corresponding labeled 2‐[^13^CD~3~]‐2,2,6‐trimethylcyclohexanone 4 in good yield. Further functionalization of 4