Integration of GC/MS Instrumentation into the Undergraduate Laboratory: Separation and Identification of Fatty Acids in Commercial Fats and Oils

Separation and identification of unsatur

Separation and identification of unsaturated fatty acid isomers in blood serum and therapeutic oil preparations in the form of their oxazoline derivatives by GC-MS

✍ Liebich, Hartmut M. ;Schmieder, Norbert ;Wahl, Hans Günther ;Wöll, Josef 📂 Article 📅 1994 🏛 John Wiley and Sons 🌐 English ⚖ 255 KB 👁 1 views

## Abstract Fatty acids from blood serum lipids and fish oil preparations are derivatized with 2‐amino‐2‐methyl‐1‐propanol to form 2‐substituted 4,4‐dimethyloxazolines. The derivatives are separated on a 25 m × 0.25 mm FFAP column and identified by mass spectrometry using electron impact ionization