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Influence of variations in the chemical structure of heparin on its anticoagulant and anti-factor Xa activities

✍ Scribed by L. Ayotte; J.C. Lormeau; A.S. Perlin

Book ID
119034712
Publisher
Elsevier Science
Year
1981
Tongue
English
Weight
438 KB
Volume
22
Category
Article
ISSN
0049-3848

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Synthesis of an N-Acetylated Heparin Pen
Synthesis of an N-Acetylated Heparin Pentasaccharide and its anticoagulant activity in comparison with the heparin pentasaccharide with high anti-factor-Xa activity
✍ Hans Peter Wessel; Ludvik Labler; Thomas B. Tschopp πŸ“‚ Article πŸ“… 1989 πŸ› John Wiley and Sons 🌐 German βš– 714 KB

The synthesis of tri-N-acetylated heparin pentasaccharide 2 is described. It was assembled from five suitably blocked monosaccharide units (S7). Glucuronic-acid building block 4 was prepared from glucose by direct Jones oxidation of the 6-0-trityl derivative 18. The resulting acid 16 was esterified