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Effect of the desulfation of heparin on its anticoagulant and anti-proliferative activity

✍ Scribed by Roberta Tiozzo; Maria Rita Cingi; Daniela Reggiani; Tiziana Andreoli; Sebastiano Calandra; Maria Rita Milani; Silvano Piani; Egidio Marchi; Miriam Barbanti

Book ID
116086411
Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
529 KB
Volume
70
Category
Article
ISSN
0049-3848

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Synthesis of an N-Acetylated Heparin Pen
Synthesis of an N-Acetylated Heparin Pentasaccharide and its anticoagulant activity in comparison with the heparin pentasaccharide with high anti-factor-Xa activity
✍ Hans Peter Wessel; Ludvik Labler; Thomas B. Tschopp πŸ“‚ Article πŸ“… 1989 πŸ› John Wiley and Sons 🌐 German βš– 714 KB

The synthesis of tri-N-acetylated heparin pentasaccharide 2 is described. It was assembled from five suitably blocked monosaccharide units (S7). Glucuronic-acid building block 4 was prepared from glucose by direct Jones oxidation of the 6-0-trityl derivative 18. The resulting acid 16 was esterified