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Improvements of the total synthesis of monocillin I and radicicol via Miyaura–Suzuki couplings

✍ Scribed by Isabelle Tichkowsky; Robert Lett

Book ID
104251132
Publisher
Elsevier Science
Year
2002
Tongue
French
Weight
314 KB
Volume
43
Category
Article
ISSN
0040-4039

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Convergent stereospecific total synthesi
Convergent stereospecific total synthesis of monocillin I and radicicol: some simplifications and improvements
✍ Isabelle Tichkowsky; Robert Lett 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 304 KB

A much improved and reliable access to the macrolide 9, key-intermediate in our synthesis of monocillin I and radicicol is reported, via a modification of our first synthesis. The formation of the conjugated E,Z-dienone trans-epoxide is now achieved in a much higher yield, in a stereospecific reacti